Metal Thickness Measurements

Metal thin films find diverse applications across a wide spectrum of industries. Metal thin films play a pivotal role in such industries as medical device manufacturing, aerospace industry, home goods, jewelry, semiconductor industries, and so many more. Ensuring quality control over metal thin film coatings is critical and essential for manufacturers. Filmetrics® offers a range of precise measurement solutions for assessing metal film thickness:

Profilometry

An Easy Method for the Measurement of Metal Thickness Profilm3D optical profilometer

Profilometry is a common and easily applicable method for metal film thickness measurements. All that is needed is a step from an uncoated to a metal-coated area to determine the step height and therewith the metal thickness. With profilometry, there is little need to know specifics about the material under investigation, and the maximum measurable thickness is only restricted by the maximum measurable thickness of the optical profiler used. The step-height accuracy in profilometry depends on the vertical resolution of the profiler. In the case of the Filmetrics Profilm3D® optical profilometer, the accuracy is 0.7% for an 8 µm step – which means 56 nm!

Sheet Resistance

Two Methods for Measuring Metal Film Thickness and Sheet Resistance

R50 sheet resistance mapping tool Contact four-point probe and non-contact eddy current probe are two methods for measuring metal film thickness and sheet resistance. A conductive sample or conductive film (and even buried or backside metal layers!) can be measured and mapped using one of the R50-Series sheet resistance mapping tools. By applying a known resistivity value either from the films library or custom supplied by the user, sheet resistance data can quickly be converted to metal film thickness maps. A large Z clearance and ± 1% accuracy ensure reliable measurement for a wide variety of sample types.

Spectral Transmittance (ST)

Metal Thickness Measurement for Very Thin Metal Films

For very thin metal films, spectral transmittance (ST) measurements are an alternative and less expensive way to measure metal film thickness. For this kind of metal thickness measurement, Filmetrics offers the F10-T. For ST measurements, the maximum measureable thickness depends strongly on the metal at hand (see table). However, there are a few limitations to this approach of metal thin film thickness analysis. For one, the substrate material must be transparent. For another, the optical constants of the material under investigation must be known to get accurate results. Often, this is uncritical because Filmetrics provides a large database of material data files with its instruments. If, on the other hand, the material’s properties are unknown or changing on a regular basis (e.g. if coating process parameters are changed occasionally), the sole measurement of ST is not enough. In this case, the following approach of combined spectral transmittance and spectral reflectance is more suited.

Combination of Spectral Transmittance and Spectral Reflectance (ST/SR)

Metal Thickness Measurements of Materials with Unknown Optical Properties F10-RT

If the optical properties of the material are unknown, a simultaneous measurement of spectral transmittance and reflectance can be used to determine the optical constants and to measure the film’s thickness in the same process. In this case, the measurable thickness range is about half of ST measurements. The instrument of choice for this is Filmetrics’ F10-RT reflectometer, which is priced about the same as our Profilm3D optical profiler.


Summary of the Three Metal Thickness Measurement Methods:

STYLUS PROFILOMETRY ST ST/SR
Suitable Instruments Profilm3D F10-RT F10-RT
Thickness Range 50nm-10mm see table below contact us
Material optical properties required? No Yes No
Transparent substrate required? No Yes Yes

Examples of Maximum Measurable Thickness Using Spectral Transmittance:

Metal Maximum Measurable Thickness by Transmittance Approx. %T Peak Position
Ag (Silver) 360nm 320nm
Al (Aluminium) 53nm 900nm
Au (Gold) 200nm 500nm
Cu (Copper) 135nm 575nm
Nb (Niobium) 135nm 750nm
Ti (Titanium) 260nm 1700nm
W (Tungsten) 133nm 1500nm

Metal Thin Film Thickness Measurement Example

This particular sample was a thin film of aluminum on a glass substrate. In order to solve for thickness as well as optical constants, measurements were taken on our F10-RT system, which combines reflectance and transmittance at normal incidence. Through the use of our “No Model” model, we measured the thickness and optical constants of this metal film, all with a single mouse-click.

Measurement Set Up

F10-RT

Measurement Result